CHEM – 617 Advanced Spectroscopy –II (Cr.03)

Mass Spectroscopy: Principle of Mass spectroscopy, Instrumentation in details, Quantitative

and Qualitative application in analytical chemistry. X-rays Spectroscopy: Nature and

production of X-rays, X-rays absorption, X-rays emission, Instrumentation, X-rays

fluorescence analysis, Diffraction studies single crystal analysis

Week	Topics and Readings
1.	Introduction to general Spectroscopy and Mass Spectrometry
2.	Instrumentation of Mass Spectrometry ( Sample Inlet system)
3.	Instrumentation of Mass Spectrometry ( Ionization Sources, electron ionization, chemical ionization, MALDI source)
4.	Instrumentation of Mass Spectrometry (Analyzers, Magnetic Sector, Quadrupole, Time of Flight), Detector, Electron multiplier Tube
5.	Interpretation of Mass Spectra (Alkane, alkene, aromatic compounds)
6.	Interpretation of Mass Spectra (Aldehydes, ketones carboxylic acids, alcohols)
7.	Applications of Mass spectrometry
8.	Nitrogen rule
9.	X-Ray Spectroscopy, general introduction
10.	Siegbahn Notation. IUPAC Notation
11.	Instrumentation of X-Ray Spectroscopy ( Source of X-Ray)
12.	Instrumentation of X-Ray Spectroscopy ( Filters and wavelength selection
13.	Sample Inlet and Detector
14.	X-Ray Absorption
15.	Brag’s law and its application
16.	Applications of X-Ray ( Medical radiography, security, molecular structure)
17.	X-ray Fluorescence
18	X-ray Diffraction